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Image Search Results
Journal: Chemistry of Materials
Article Title: Environmental and Thermal Stability of Chemically Exfoliated LixMoS2 for Lithium–Sulfur Batteries
doi: 10.1021/acs.chemmater.4c00674
Figure Lengend Snippet: Figure 1. Material characterization of 1T MoS2 and LixMoS2 nanosheets in comparison to bulk 2H MoS2. (a) Raman spectra showing E2g 1 (in- plane; 382 cm−1) and A1g (out-of-plane; 406 cm−1) peaks, 1T features (J1, J2, and J3 peaks at 153, 220, and 325 cm−1) and c peak at 250 cm−1. (b) XRD patterns showing a new (001) peak at 7.8°, suggesting 2H to 1T phase transformation and an increase in interlayer spacing. (c) Deconvoluted high-resolution Mo 3d XPS spectra, showing ∼74% 1T phase concentration for 1T MoS2 nanosheets, and ∼79% for LixMoS2 nanosheets.
Article Snippet: ■ MATERIAL CHARACTERIZATION The materials were characterized by Raman spectroscopy (Renishaw InVia using a 514 nm laser beam),
Techniques: Comparison, Transformation Assay, Concentration Assay
Journal: Chemistry of Materials
Article Title: Environmental and Thermal Stability of Chemically Exfoliated LixMoS2 for Lithium–Sulfur Batteries
doi: 10.1021/acs.chemmater.4c00674
Figure Lengend Snippet: Figure 5. Comparison of (a) XRD patterns and (b) Raman spectra of as-synthesized LixMoS2 nanosheets and LixMoS2 exposed to dry and humid air for 48 h. LixMoS2 exposed to humid air shows peaks at 19.8 and 21.1°, which are characteristic peaks of Li2MoO4. The Raman spectra of both samples show features unique to the 1T phase. However, the sample exposed to humid air lost intensity for J1 and J3 and did not retain the c peak located at 250 cm−1.
Article Snippet: ■ MATERIAL CHARACTERIZATION The materials were characterized by Raman spectroscopy (Renishaw InVia using a 514 nm laser beam),
Techniques: Comparison, Synthesized